[1]孟瑶瑶,王俊淇,王杰,等. 狮头柑籽油提取工艺及脂肪酸组成研究[J].西北林学院学报,2019,34(2):199-205.[doi:10.3969/j.issn.1001-7461.2019.02.30]
 MENG Yao-yao,WANG Jun-qi,WANG Jie,et al. Extraction Technology and Fatty Acid Composition of Shitougan Seed Oil[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2019,34(2):199-205.[doi:10.3969/j.issn.1001-7461.2019.02.30]
点击复制

 狮头柑籽油提取工艺及脂肪酸组成研究()
分享到:

《西北林学院学报》[ISSN:1001-7461/CN:61-1202/S]

卷:
第34卷
期数:
2019年第2期
页码:
199-205
栏目:
出版日期:
2019-03-31

文章信息/Info

Title:
 Extraction Technology and Fatty Acid Composition of Shitougan Seed Oil
文章编号:
1001-7461(2019)02-0199-07
作者:
 孟瑶瑶12王俊淇1王杰1刘玉垠1鲁周民1*
 (1.西北农林科技大学 林学院,陕西 杨陵 712100;2.山东黄河三角洲国家级自然保护区管理局,山东 东营 257091)
Author(s):
 MENG Yao-yao12WANG Jun-qi1WANG Jie1LIU Yu-yin1LU Zhou-min1
 (1.College of Forestry,Northwest A&F University,Yangling 712100,Shaanxi,China; 2.Shandong Yellow River Delta National Nature Reserve,Dongying 257091,Shandong,China)
关键词:
 狮头柑籽响应面优化法气相色谱-质谱法(GC-MS)脂肪酸组成
Keywords:
 shitougan seed response surface optimization gas chromatography-mass spectrometry fatty acid composition
分类号:
R284.2
DOI:
10.3969/j.issn.1001-7461.2019.02.30
文献标志码:
A
摘要:
 为探索狮头柑籽油的提取工艺,给生产利用提供理论依据及技术方法。在优选了提取溶剂及单因素试验基础上,对料液比、提取时间、提取温度3因素运用中心组合(Box-Benhnken)试验设计进行狮头柑籽油提取技术研究。提取狮头柑籽油的适宜溶剂为乙醚;确定了狮头柑籽油索氏提取的优化工艺条件为:料液比1∶100(g/mL),提取温度49℃,提取时间7 h,并拟合出狮头柑籽油得率的预测模型(R2=0.985 9)。采用气相色谱-质谱联用法(gas chromatography-mass spectrometry,GC-MS)鉴定出狮头柑籽油中的脂肪酸组分,包括油酸、亚油酸、棕榈酸、花生酸等9种,其中亚油酸含量最高,达72.00%。研究提出的工艺技术可用于狮头柑籽油的提取生产,出油率可达37.61%。
Abstract:
 This study aimed to explore the extraction technology of seed oil of Citrus reticulata cv.Manau Gan fruit (shitougan) to provide theoretical basis and technical methods for its production and utilization.Based on optimizing the extraction solvent and the result of single factor experiments,three factors,including solid-liquid ratio,extraction time,and extraction temperature were applied to the Box-Benhnken design principle.The results showed that diethyl ether was the suitable solvent for extracting shitougan seed oil,and the otimize process conditions of extraction shitougan seed oil were obtained as solid-liquid ratios:1∶100(g/mL),extraction temperature: 49℃,extraction time: 7 h.The prediction model for the yield of shitougan seed oil (R2=0.985 9) was simulated.Fatty acid composition of shitougan seed oil was analyze by gas chromatography-mass spectrometry(GC-MS).Nine kinds of fatty acid component were identified,including oleic acid,linoleic acid,palmitic acid and arachidic acid,etc.The highest fatty acid component was linoleic acid (72.00%).The research and technology proposed could be used for the extraction and production of shitougan seed oil,with the oil yield of 37.61%.

相似文献/References:

[1]李亚藏,梁彦兰,王庆成. 铅对山梨和山荆子光合作用和叶绿素荧光特性的影响[J].西北林学院学报,2012,27(05):21.
 LI Ya-cang,LIANG Yan-lan,WANG Qing-cheng. Influence of Pb on Photosynthesis and Chlorophyll Fluorescence Characteristics in Pyrus ussuriensis and Malus baccata [J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2012,27(2):21.
[2]张小咏,李佳,杨艳昭,等. 基于SWAT模型的长江源区径流模拟[J].西北林学院学报,2012,27(05):38.
 ZHANG Xiao-yong,LI Jia,YANG Yan-zhao,et al. Runoff Simulation of the Catchment of the Headwaters of the Yangtze River Based on SWAT Model[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2012,27(2):38.
[3]杨红旗,陈广辉,王金林. PVAc改性酚醛树脂制备铝木复合材料研究[J].西北林学院学报,2013,28(01):170.[doi:10.3969/j.issn.1001-7461.2013.01.34]
 YANG Hong-qi,CHEN Guang-hui,WANG Jin-lin. PF Adhesive Modified by PVAc for Manufacturing Technology of Decorative Fiberboard with Aluminum Foils[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2013,28(2):170.[doi:10.3969/j.issn.1001-7461.2013.01.34]
[4]江涛,李秀荣,谢延军,等. 微波预处理对巨尾桉木材渗透性的影响[J].西北林学院学报,2013,28(01):174.[doi:10.3969/j.issn.1001-7461.2013.01.35]
 JIANG Tao,LI Xiu-rong,XIE Yan-jun,et al. Effects of Microwave Pretreatment on the Permeability of Eucalyptus grandis×Eucalyptus urophylla[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2013,28(2):174.[doi:10.3969/j.issn.1001-7461.2013.01.35]
[5]牛晓霆,王逢瑚,曹新民. 明清家具匠师原木下料的工艺原则及措施[J].西北林学院学报,2013,28(01):178.[doi:10.3969/j.issn.1001-7461.2013.01.36]
 NIU Xiao-ting,WANG Feng-hu,CAO Xin-min. Techniques and Principles of Log Cuttings of Furniture Makers in Ming and Qing Dynasties[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2013,28(2):178.[doi:10.3969/j.issn.1001-7461.2013.01.36]
[6]吕金阳,覃卓凯,舒辉,等. 银杉木材构造美学价值[J].西北林学院学报,2013,28(01):183.[doi:10.3969/j.issn.1001-7461.2013.01.37]
 LV Jin-yang,QIN Zhuo-kai,SHU Hui,et al. Esthetical Values in Wood Structure of Cathaya argyrophylla[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2013,28(2):183.[doi:10.3969/j.issn.1001-7461.2013.01.37]
[7]杨艳红,张海敏,孙景荣. 基于传统文化视角的现代家具设计探析[J].西北林学院学报,2013,28(01):188.[doi:10.3969/j.issn.1001-7461.2013.01.38]
 YANG Yan-hong,ZHANG Hai-min,SUN Jing-rong. Study of Modern Furniture Design Based on Traditional Culture[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2013,28(2):188.[doi:10.3969/j.issn.1001-7461.2013.01.38]
[8]黄圣游,叶喜. 新中式家具“中式”传统的界定[J].西北林学院学报,2013,28(01):192.[doi:10.3969/j.issn.1001-7461.2013.01.39]
 HUANG Sheng-You,YE Xi. Definition of Traditional Element in New Chinese Style Furniture[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2013,28(2):192.[doi:10.3969/j.issn.1001-7461.2013.01.39]
[9]韩维生,赵明磊,王宏斌. 基于阈限理论的设计尺度体系[J].西北林学院学报,2013,28(01):197.[doi:10.3969/j.issn.1001-7461.2013.01.40]
 HAN Wei-sheng,ZHAO Ming-lei,WANG Hong-bin. Design Scale System Based on Threshold Theory[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2013,28(2):197.[doi:10.3969/j.issn.1001-7461.2013.01.40]
[10]宋杰,侯建军,申黎明. 按摩椅按摩头包覆层对按摩舒适性的影响[J].西北林学院学报,2013,28(01):202.[doi:10.3969/j.issn.1001-7461.2013.01.41]
 SONG Jie,HOU Jian-jun,SHEN Li-ming. Influence of Massager Coat Layer of Massage Chairs on the Degree of Comfort[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2013,28(2):202.[doi:10.3969/j.issn.1001-7461.2013.01.41]

备注/Memo

备注/Memo:
 收稿日期:2018-05-18修回日期:2018-08-20
基金项目:财政部“以大学为依托的农业科技推广模式建设”项目(XTG2017014)。
作者简介:孟瑶瑶,女,在读硕士,研究方向:植物资源利用。E-mail:861602335@qq.com
*通信作者:鲁周民,男,研究员,博士生导师,研究方向:经济林果品加工。E-mail:lzm@nwsuaf.edu.cn
更新日期/Last Update: