[1]韩爱芝,白红进,耿会玲,等. 响应面法优化超声辅助提取黑果枸杞叶片总黄酮的工艺研究[J].西北林学院学报,2013,28(01):114-118.[doi:10.3969/j.issn.1001-7461.2013.01.22]
 HAN Ai-zhi,BAI Hong-jin,GENG Hui-ling,et al. Optimization of Ultrasound-assisted Extraction of Total Flavonoids from Lycium ruthenicum Leaves by Response Surface Methodology[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2013,28(01):114-118.[doi:10.3969/j.issn.1001-7461.2013.01.22]
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 响应面法优化超声辅助提取黑果枸杞叶片总黄酮的工艺研究()
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《西北林学院学报》[ISSN:1001-7461/CN:61-1202/S]

卷:
第28卷
期数:
2013年01期
页码:
114-118
栏目:
出版日期:
2013-01-30

文章信息/Info

Title:
 Optimization of Ultrasound-assisted Extraction of Total Flavonoids from Lycium ruthenicum Leaves by Response Surface Methodology
文章编号:
1001-7461(2013)01-0114-05
作者:
 韩爱芝白红进耿会玲孟庆艳
 (1.塔里木大学 生命科学学院,新疆 阿拉尔 843300;2.新疆生产建设兵团塔里木盆地生物资源保护与利用重点实验室,新疆 阿拉尔 843300;3.西北农林科技大学 理学院,陕西 杨陵 71210)
Author(s):
 HAN Ai-zhiBAI Hong-jinGENG Hui-lingMENG Qing-yan
 (1.Colleng of Life Science,Tarim University,Alaer, Xinjiang 843300,China;2. Key Laboratory of Protection & Utilization of Biological Resources in Tarim Basin of Xinjiang Production and Construction Corps,Alaer,Xinjiang 843300,China;3.College of Science,Northwest A&F University,Yangling,Shaanxi 712100,China)
关键词:
 黑果枸杞叶 响应面法 超声波辅助提取 总黄酮
Keywords:
Lycium ruthenicum leafresponse surface methodultrasound-assisted extractiontotal flavonoid
分类号:
S793.9
DOI:
10.3969/j.issn.1001-7461.2013.01.22
文献标志码:
A
摘要:
 采用单因素试验,研究乙醇浓度、料液比、超声时间、超声温度及超声功率对总黄酮提取率的影响,依据Box-Behnken的中心组合设计,采用四因素三水平响应面法优化从黑果枸杞叶中提取总黄酮的最佳工艺条件。结果表明: 最佳工艺为,乙醇提取浓度为70%,超声功率400 W,料液比为1∶25,超声提取温度58℃,黑果枸杞叶片总黄酮的平均得率为1.62 %。与理论预测值的相对误差为1.22 %。说明响应面法优化超声提取黑果枸杞叶片总黄酮的工艺条件稳定可行。
Abstract:
 The technology of the ultrasound-assisted extraction of total flavonoids from Lycium ruthenicum leaves was optimized by using the response surface methodology (RSM) to examine the effects of variables on the extraction yields,such as ethanol concentration,solid-liquid ratio,time,temperature,and the ultrasonic power.The optimum extraction conditions were as follows:ethanol concentration: 70%,ultrasound power:400 W,material to liquid ratio:1∶25,and extraction temperature: 58 ℃.Under the optimum conditions,the extraction yield of total flavonoids was 1.62 %.The relative error with the theoretical value was 1.22 %.The optimized process obtained from RSM was reliable,stable,and practical.

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备注/Memo

备注/Memo:
 收稿日期:2012-03-30 修回日期:2012-06-27
基金项目:新疆生产建设兵团高新技术研究发展计划项目( 2007GX20);塔里木大学校长基金重点项目( TDZKZD05002)。
作者简介:韩爱芝,女,硕士研究生,研究方向:天然产物分子结构及功能。E-mail:haz2099@163.com
*通信作者:白红进,男,教授,硕士生导师,研究方向:天然产物分子结构及功能。E-mail:bhj67@163.com
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