[1]褚学英.火棘红色素的大孔吸附树脂分离纯化工艺研究火棘红色素的大孔吸附树脂分离纯化工艺研究[J].西北林学院学报,2009,24(02):115-117.
　CHU Xue ying.Absorption and Separation of Red Pigments by Macroporous Resin from Pyracantha fortuneana[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2009,24(02):115-117.
点击复制

火棘红色素的大孔吸附树脂分离纯化工艺研究火棘红色素的大孔吸附树脂分离纯化工艺研究()
分享到：

《西北林学院学报》[ISSN:1001-7461/CN:61-1202/S]

卷:
第24卷
期数:
2009年02期
页码:
115-117
栏目:
林产化学
出版日期:
2009-03-30

文章信息/Info

Title:
Absorption and Separation of Red Pigments by Macroporous Resin from Pyracantha fortuneana
作者:
褚学英
（南阳师范学院，河南 南阳 473061）
Author(s):
CHU Xueying
(Nanyang Normal University，Nanyang, Henan 473061, China)
关键词:
火棘红色素; 提取; 精制
Keywords:
red pigment of Pyracantha fortuneana; extraction ; refinement
分类号:
S793.908
文献标志码:
A
摘要:
对火棘红色素的提取和精制工艺进行研究。结果表明，火棘红色素最佳提取条件为以pH3.0的80%乙醇作浸提剂，提取温度50℃，提取时间3 h，固液配比1∶40；用X5大孔吸附树脂对色素进行精制，以树脂柱径高比1∶15、流速3 mL·min-1，pH3.0、色素液浓度1 g·L-1为最佳吸附条件，色素的吸附量可达0.037 15 g·mL-1湿树脂体积；而以95%乙醇做洗脱液，在pH2.0、流速5 mL·min-13倍于柱床体积的洗脱液条件下解吸效果最佳。
Abstract:
The extraction and purification technology of the red pigments from Pyracantha fortuneana is investigated by orthogonal design method. The preferable extraction conditions were as follows: solvent 80% ethanol, ratio of solvent to material 40 ,pH 3.0, temperature 50℃, time of extraction 3 h, the purification conditions for adsorption were X5 macroporous resin, ratio of height to diameter of the resin loaded in the column 15, rate of elution 3 mL·min-1, pH3.0, concentration of the extract being separated 1 g·L-1. The amount of adsorption of the extract reached 0 .037 15 g·mL-1 wet resin. The elution conditions were 95% ethanol as solvent, pH 2.0, elution rate 5 mL·min-1, 3 times of the resin volume of eluent.

相似文献/References:

[1]周郑坤,周文明通讯作者：周文明(9),男,等.胖大海水溶性多糖的提取[J].西北林学院学报,2006,21(04):129.
　ZHOU Zhengkun,ZHOU Wenming,HE Mingyu,et al.Study on Extraction of Watersoluble Polysaccharide of Sterculia lychnophora[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2006,21(02):129.
[2]吴静,李永华,何松林,等.牡丹根系RNA提取方法的比较研究[J].西北林学院学报,2010,25(05):60.
[3]龚晓武,李炳奇,刘丹丹,等.红景天黄酮提取及其抗氧化活性研究[J].西北林学院学报,2011,26(03):136.
[4]王丽,苏印泉,张强,等. 光叶楮叶蛋白提取工艺优化和氨基酸分析研究[J].西北林学院学报,2012,27(02):137.
　WANG Li,SU Yin-quan,ZHANG Qiang,et al. Optimization of Extraction Technology and Amino Acid Analysis of Protein Extracted from Broussonetia Leaf[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2012,27(02):137.
[5]孙璐宏,鲁周民,张丽,等.植物基因组DNA提取与纯化研究进展[J].西北林学院学报,2010,25(06):102.
[6]欧阳辉,余佶,张永康,等.湘西椪柑果皮中果胶提取工艺优化研究[J].西北林学院学报,2011,26(02):185.
[7]吴洪新,陈晨. 尖叶胡枝子总黄酮提取与纯化研究[J].西北林学院学报,2014,29(02):196.[doi:doi:10.3969/j.issn.1001-7461.2014.02.35]
　WU Hong-xin,CHNE Chen. Extraction and isolation of Flavonoids From Lespedeza hedysaroides[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2014,29(02):196.[doi:doi:10.3969/j.issn.1001-7461.2014.02.35]
[8]王晓林,钟方丽*,薛健飞,等. 微波协同酶法提取刺玫叶总黄酮工艺研究[J].西北林学院学报,2015,30(04):246.[doi:doi:10.3969/j.issn.1001-7461.2015.04.40]
　WANG Xiao-lin,ZHONG Fang-li*,XUE Jian-fei,et al. Extraction Technology of Total Flavonoids in the Leaves of Rosa davurica with Microwave Assisted Enzymes Method[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2015,30(02):246.[doi:doi:10.3969/j.issn.1001-7461.2015.04.40]
[9]张珊珊,孟园,林文树*. 基于三维激光扫描技术的单木参数提取精度研究[J].西北林学院学报,2017,32(5):189.[doi:10.3969/j.issn.1001-7461.2017.05.32]
　ZHANG Shan-shan,MENG Yuan,LIN Wen-shu*. Extraction Precision of Forest Parameters at Single-tree Level Based on 3D Laser Scanning Technology[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2017,32(02):189.[doi:10.3969/j.issn.1001-7461.2017.05.32]
[10]周宇波,李霞飞,高岳芳*,等. 水热法提取龙井长叶中茶多糖工艺优化研究[J].西北林学院学报,2018,33(1):207.[doi:10.3969/j.issn.1001-7461.2018.01.34]
　ZHOU Yu-bo,LI Xia-fei,GAO Yue-fang*,et al. Optimization of Extraction Technology of Polysaccharides by Hydrothermal Method from Longjing-changye (Camellia sinensis)[J].JOURNAL OF NORTHWEST FORESTRY UNIVERSITY,2018,33(02):207.[doi:10.3969/j.issn.1001-7461.2018.01.34]

备注/Memo

备注/Memo:
收稿日期：20080127修回日期：20080305作者简介：褚学英，女，实验师，研究方向：微生物和资源生物学。
更新日期/Last Update: